Obtención y caracterización de nanopartículas de plata soportadas en fibra de algodón

J. López Iturbe; A. R. Vilchis Nestor; V. Sánchez Mendieta; M. Avalos Borja

Vol. 26 No. 3 (2013), Research Papers

Vol. 26 No. 3 (2013)

Production and characterization of silver nanoparticles supported on cotton fibers

Research Papers

Published 2013-09-15

J. López Iturbe⁺⁻
A. R. Vilchis Nestor⁺⁻
V. Sánchez Mendieta⁺⁻
M. Avalos Borja⁺⁻

J. López Iturbe

Postgrado en Ciencia de Materiales, Facultad de Química, Universidad Autónoma del Estado de México

A. R. Vilchis Nestor

Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, (CCIQS)

V. Sánchez Mendieta

Facultad de Química, Universidad Autónoma del Estado de México

M. Avalos Borja

Centro de Nanociencias y Nanotecnologia, Universidad Nacional Autónoma de México

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Keywords

Bioreduction
Nanoparticles
Natural fibers
Biocomposites. Bioreducción
Nanopartículas
Fibras naturales
Biocompositos.

How to Cite

López Iturbe, J., Vilchis Nestor, A. R., Sánchez Mendieta, V., & Avalos Borja, M. (2013). Production and characterization of silver nanoparticles supported on cotton fibers. Superficies Y Vacío, 26(3), 73-78. Retrieved from https://superficiesyvacio.smctsm.org.mx/index.php/SyV/article/view/157

Abstract

In this work, silver nanoparticles biocomposite by using cotton fiber as support and Camellia sinensis as reducing agent were prepared. For biocomposite preparation, anionically charged cotton fibers were first immersed in a silver ions solution. Later, a second immersion of the fibers in a Camellia sinensis solution was done. The biocomposites were characterized by infrared spectroscopy in order to identify structural changes of cellulose. The fibers were observed in Field Emission Scanning Electron Microscopy (FE-SEM) and Field Emission Transmission Electron Microscopy (FETEM) in order to determine the surface impregnation of the fibers with Ag nanoparticles and the grain size distribution respectively, finding average sizes of 5 y 11 nm for two different probes. Finally, the binding energies of the reduced silver as measured by X-ray photoelectron spectroscopy (XPS) show that metallic silver (Ag0) and a complex of silver and oxygen (Ag-O) were presented on the fibers.

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