Effect of thermal treatment ambient gas and Eu doping on the structural properties of electrospun TiO2 nanofibers
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Keywords

Nanofibers
TiO2
Phase transformation. Nanofibras
TiO2
Transformación de fase.

How to Cite

Cruz González, N., Fernández Muñoz, J. L., Zapata Torres, M., & García Hipólito, M. (2013). Effect of thermal treatment ambient gas and Eu doping on the structural properties of electrospun TiO2 nanofibers. Superficies Y Vacío, 26(3), 111-116. Retrieved from https://superficiesyvacio.smctsm.org.mx/index.php/SyV/article/view/164

Abstract

In this work we studied the influence of annealing atmosphere and Eu doping in the structural transformation on TiO2nanofibers, grown by electrospinning technique. The TiO2 samples were annealing to different temperatures under controlled atmosphere of Nitrogen and air. The TiO2:Eu samples were annealing in air atmosphere. The morphology has been studied by Scanning Electron Microscopy (SEM) and crystalline structure was analyzed by X-Ray Diffraction (DRX) and Raman. The nitrogen atmosphere promotes at lower temperatures the anatasa to rutilo transformation, compared with the air atmosphere. The Eu impurification increases the annealing temperature for the anatasa to rutile transformation.
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References

Li D, Xia Y; Nano Letters 3, 555 (2003).

Viswanathamurthi P, Bhattarai N, Kin CK, Kim HY, Lee DR; Inorg Chem Commun 7, 679 (2004).

Akira Fijishima, Xintong Zhang, Donald A. Tryk: Surface Science Reports 63, 515 (2008).

Lee KM, Suryanarayanan V, Ho KC; Sol Energy Mater Sol Cells 91, 1416 (2007).

Zhang X, Xu S, Han G; Mater Lett 63, 1761 (2009).

Chen X, Mao SS; J. Nanosci. Nanotechnol 6, 906 (2006).

Li X, Xiong Y, Li Z,Xie Y; Inorg. Chem. 45, 3493 (2006).

Cozzoli PD, Kornowski A, Weller H; J. Am. Chem Soc. 125 14539 (2003).

Li D, Xia Y; Nano Lett. 3, 555 (2003).

Liu Z, Zhang X, Nishimoto S, Jin M, Rryk DA, Marakami T, Fujishima A; J. Phys. Chem. C 112, 253 (2007).

Chen Y, Tian G, Ren Z, Tian C, Pan K, Zhou W, Fu H; Eur. J. Inorg. Chem 2011, 754 (2011).

Almquist CB, Biswas P; J. Catal. 212, 145 (2002).

Sclafani A., Herrmann J.M.; J. Phys. Chem 100, 13655 (1996).

Hadjiivanov K.I., Klissurski D.G.; Chem. Soc. Rev. 25, (1996) 61.

Altangerel Amarjargal, Leonard D. Tijing, Cheol Sang Kim: Ceramics International 38, 6365 (2012).

Setiawati E, Kawano K; Jornal of Alloys and Compounds 451, 293 (2008).

Tobaldi DM, Sever Skapin A, Pullar RC, Seabra MP, Labrincha JA; Ceramics International 39, 2619 (2013).

Ilaria Cacciotti, Alessandra Blanco, Giuseppe Pezzotti, Gualtiero Gusmano, Chemical Engineering Journal 166, 751 (211).

Porto SPS, Fluery PA, Damen TC; Phys. Rev. 154, 522 (1967).

Spurr RA, Myers H; Anal. Chem. 29, 760 (1957).