Synthesis of titanium oxide nanoparticles by plasma

Authors

  • F. González Salgado Departamento de Física, Instituto Nacional de Investigaciones Nucleares. Departamento de Posgrado, Instituto Tecnológico de Toluca.
  • M. G. Olayo Departamento de Física, Instituto Nacional de Investigaciones Nucleares
  • G. J. Cruz Departamento de Física, Instituto Nacional de Investigaciones Nucleares. Departamento de Posgrado, Instituto Tecnológico de Toluca.
  • L. M. Gómez Departamento de Física, Instituto Nacional de Investigaciones Nucleares. Posgrado en Ciencia de Materiales, Facultad de Química, Universidad Autónoma del Estado de México.
  • E. Ordoñez Departamento de Química, Instituto Nacional de Investigaciones Nucleares
  • G. García Rosales Departamento de Posgrado, Instituto Tecnológico de Toluca

Keywords:

Titanium oxide, Nanoparticles, Plasma

Abstract

This work presents a study about the evolution of titanium oxide particles synthesized with glow discharges of water and Tetra Titanium Propoxide (TTP). The syntheses involved sequential changes of TTP from solid, liquid and vapor phases under resistive glow discharges at 13.56 MHz, 0.5-0.8 mbar and 100 W with reaction times between 60 and 240 min. The reaction of TTP and water between the electrodes originated titanium oxide powder composed of white particles with diameter between 106 and 695 nm and different geometries depending on the time of synthesis. These materials may have environmental applications in the sorption of toxic contaminants.

References

. X. Fan, L. Lin, B. P. Messersmith. Composites Science and Technology. 66, 1195 (2006).

. H. Yang , K. Zhang, R. Shi, X. Li, X. Dong, Y. Yu., Journal of Alloys and Compounds. 41, 302 (2006).

. S. Pavasupree, S. Ngamsinlapasathian, M. Nakajima, Y. Suzuki, S. Yoshikawa. Journal of Photochemistry and Photobiology A: Chemistry. 184, 163 (2006).

. J. Aguado, R. van Grieken, M.J. López-Muñoz and J. Marugán. Catalysis Today. 75, 95 (2002).

. F. Fresno, J. M. Coronado, D. Tudela, J. Soria. Applied Catalysis B: Environmental. 55 (3), 159 (2005).

. D.L. Liao, G.S.Wu, B.Q. Liao. Colloids and Surfaces A: Physicochem. Eng. Aspects. 348, 270 (2009).

. B. F. Cottam, S. Krishnadasan, A. J. deMello, John C. deMello and M. S. P. Shaffer. The Royal Society of Chemistry. 7, 167 (2007).

. R. Szabova, L. Cernákova, M. Wolfová, M. Cernák. Acta Chimica. Slovaca. 2(1), 70 (2009).

. X. Chen, M. Schriver, T. Suen and S. S. Mao. Thin Solid Films. 515(4), 8511(2007).

. S. Pavasupree, Y. Suzuki, S. Yoshikawa and R. Kawahata. J. Solid State Chemistry. 178(10), 3110(2005).

. S. Pavasupree, S. Ngamsinlapasathian, M. Nakajima, Y. Susuki, S. Yoshikawa. J. Photochem. Photobiol. A: Chem. 184, 163 (2006).

. J. Ani, S. Savithri, G. Surender. Aerosol and Air Quality Research. 5, 1(2005).

. G.J. Cruz, M.G. Olayo, O.G López, L.M. Gómez, J. Morales, R. Olayo. Polymer. 51, 4314 (2010).

. R. Asmatulu, A. Karthikeyan, D. C. Bell, S. Ramanathana and M. J. Aziz. Journal of Materials Science. 44, 4613 (2009).

. M.G. Olayo, J. Morales, G.J. Cruz, S.R. Barocio, R. Olayo. Journal of Polymer Science, Part B: Polymer Physics. 41, 1501 (2003).

. W. Li, S. Ismat, M. Sung, C.P. Huang. J. Vac. Sci. Technol. B. 20, 2303 (2002).

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Published

2012-03-15

How to Cite

González Salgado, F., Olayo, M. G., Cruz, G. J., Gómez, L. M., Ordoñez, E., & García Rosales, G. (2012). Synthesis of titanium oxide nanoparticles by plasma. Superficies Y Vacío, 25(1), 56–59. Retrieved from https://superficiesyvacio.smctsm.org.mx/index.php/SyV/article/view/229

Issue

Vol. 25 No. 1 (2012)

Section

Research Papers

License

©2025 by the authors; licensee SMCTSM, Mexico. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/4.0/).