Method for measuring the setting process of cement-water mixtures by electrical impedance
Vol. 37 (2024), Research Papers
Vol. 37 (2024)

Method for measuring the setting process of cement-water mixtures by electrical impedance

Research Papers
https://doi.org/10.47566/2024_syv37_1-240101
Published 2024-02-07
Eduardo Morales Sánchez
National Polytechnic Institute. CICATA-IPN Queretaro Unit
https://orcid.org/0000-0002-0855-5460
Jorge Pineda Piñón
National Polytechnic Institute. CICATA-IPN Queretaro Unit
https://orcid.org/0000-0003-1392-6534
Alejandro Manzano Ramírez
CINVESTAV-IPN, Querétaro Unit
https://orcid.org/0000-0001-7954-6978
José Mauricio López-Romero
CINVESTAV-IPN, Querétaro Unit
https://orcid.org/0000-0003-3435-9241
Marcela Gaytán Martinez
Faculty of Chemistry. UAQ
https://orcid.org/0000-0002-1168-3877
Guadalupe Omar Sánchez Vega
Universidad Tecnológica de Querétaro
https://orcid.org/0000-0001-5709-4325
Relative electrical impedance, setting process.
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Keywords

Electrical resistivity
electrical impedance
hydration
cement
setting time

How to Cite

Morales Sánchez, E., Pineda Piñón, J., Manzano Ramírez, A., López-Romero, J. M., Gaytán Martinez, M., & Sánchez Vega, G. O. (2024). Method for measuring the setting process of cement-water mixtures by electrical impedance. Superficies Y Vacío, 37, 240101. https://doi.org/10.47566/2024_syv37_1-240101
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Abstract

The setting and hardening of cement paste can be taken as the progressive hydration reaction of cement. This paper reports the findings on setting time of cement paste at early hydration by using a novel method named relative electrical impedance (REI). The novel REI method measures the relative electrical impedance between electrodes (ring shaped) embedded in the cement paste. REI measurements were conducted on cement paste samples with a water-cement ratio of 1:2 over 24 hours. REI measurements were compared with VICAT and heat latent methods for indirect validation. It was found that the proposed REI technique determined the 4 periods of the setting time process (sleeping, hydration, deceleration, and diffusion) and allowed the measurement of the sleeping period in detail. It was concluded that the novel REI method could be used as a new method to measure the setting time of cement paste in early hydration.

https://doi.org/10.47566/2024_syv37_1-240101
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