Obtaining and characterization of ZnSe nanoparticles from aqueous colloidal dispersions
Vol. 27 No. 1 (2014), Research Papers
Vol. 27 No. 1 (2014)

Obtaining and characterization of ZnSe nanoparticles from aqueous colloidal dispersions

Research Papers
Published 2014-03-15
R. Hernández
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
E. Rosendo
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
G. García
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
M. Pacio
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
T. Díaz
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
H. Juárez
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
R. Galeazzi
PDS, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla
R. Romano Trujillo
Instituto de Energías Renovables, UNAM
G. Nieto
Facultad de Ciencias Químicas, Benemérita Universidad Autónoma de Puebla
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Keywords

ZnSe
Nanoparticles
Colloidal method
Aqueous media

How to Cite

Hernández, R., Rosendo, E., García, G., Pacio, M., Díaz, T., Juárez, H., Galeazzi, R., Romano Trujillo, R., & Nieto, G. (2014). Obtaining and characterization of ZnSe nanoparticles from aqueous colloidal dispersions. Superficies Y Vacío, 27(1), 11-14. Retrieved from https://superficiesyvacio.smctsm.org.mx/index.php/SyV/article/view/147
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Abstract

Structural, morphological and compositional characterizations of zinc selenide (ZnSe) nanoparticles (NPs) are presented. ZnSe NPs have been obtained by colloidal synthesis in aqueous solution using zinc nitrate (Zn(NO3)2) and elemental selenium (Se) as precursors, sodium borohydride (NaBH4) as reducing agent, a solution of sodium hydroxide (NaOH) and pentasodium tripolyphosphate (Na5P3O10) named Extran was used as surfactant. The pH was varied from 8 to 11 and the Zn:Se molar concentration was varied from 3:1 to 1:3. A cleaning process was applied to eliminate the by-products using hydrochloric acid (HCl). ZnSe NPs exhibit a cubic zinc-blende structure. The NPs size was estimated between 4.9 nm and 3.0 nm and depends on molar concentration.
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References

A. Sadao, T. Tsunemasa, Physical Review B 43 9569 (1991).

Y. H. Chang, M. H. Chieng, C.C. Tsai, M. C. Harris Liao, F. Chen, Journal of Electronic Materials, 29, 173 (2000).

C. H. Zhang, P. B. Meng, B. Q. Yao, G. Li, Y. L. Ju, Y. Z. Wang, Laser Physics, 21, 44 (2011).

M. A. Hines, P. G. Sionnest, Nanocrystals, J Phys Chem B, 102, 3655 (1998).

K. Lin, S. J. Chang, Y. K. Su, Y. Z. Chiou, C. K. Wang, IEEE Trans Electron Devices, 52, 121 (2005).

D. H. Kim, Y. H. Lee, D. U. Lee, T. W. Kim, S. Kim, S. W. Kim, Opt Express 20, 10476 (2012).

J. Zhu, Y. Koltypin, A. Gedanken, Chem. Mater.12, 73 (2000).

L. Li, N. Pradhan, Y. Wang, X. Peng Nano Lett., 4, 2261 (2004).

D. J. Norris, N. Yao, F. T. Charnock, T. A. Kennedy, Nano Lett. 1, 3 (2001).

B. Xiang, H. Z. Zhang, G. H. Li, F. H. Yang, F. H. Su, R. M. Wang, J. Xu, G. W. Lu, X. C. Sun, Q. Zhao, D. P. Yu, Appl. Phys. Lett., 82, 3330 (2003).

J. W. Lee, S. M. Lee, Y. D. Huh, C. S. Hwang, Bull. Korean Chem. Soc., 7, 31 (2010).

C. B. Murray, S. Sun, W. Gaschler, H. Doyle, T. A. Betley, C. R. Kagan, IBM J. Res. Dev. 45, 47 (2001).

J. Chomoucka, J. Drbohlavova, P. Businova, M. Ryvolova, V. Adam, R. Kizek, J. Hubalek, Electronics Technology, 2009. ISSE 2009. 32nd International Spring Seminar on Electronics Technology (ISSE).

R. Romano-Trujillo, E. Rosendo, M. Ortega, A. M. Sanchez, J. M. Gracia, T. Diaz, G. Nieto, G. Garcia, J. A. L. Lopez, M. Pacio, Nanotechnology 23, 185602 (2012).

I. C. Baek, S. I. Seok, N. C. Pramanik, S. Jana, M. A. Lim, B. Y. Ahn, C. J. Lee, Y. J. Jeong Colloid Interface, Sci. June, 310, 163 (2007).